Technoorg Linda

Technoorg Gentle Mill
Ion Beam Workstations for preparing
highest quality (S)TEM / FIB samples

 
The Gentle Mills’ exclusive capability of producing damage-free samples at low-energy ion bombardment provides unique opportunity to study the real nanostructures in synthesized and natural materials in all fields of technical sciences and materials research.

 Fast, reliable and easy-to-use
 For cleaning, improving and postprocessing of TEM and FIB samples
 Manual (IV5) or automated (IV8) version available
 Built-in PC with user-friendly graphical interface
 

Low-Energy Ion Mills for Final Polishing
Technoorg’s Gentle Mill™ "Ion Beam Workstation" series has been designed for final polishing, easy cleaning and improving of samples previously treated in standard high- energy ion mills or FIB columns. Gentle Mill models are recommended to users who want to prepare artifact-free and almost damage-free XTEM, HRTEM or STEM samples of the best possible quality.
The Gentle Mill™ ion beam workstations operate with an outstanding patented hot-cathode low-energy ion source. The extremely low energy of the ion beam guarantees minimization of surface damage and ion beam induced amorphization. The exceptional construction of the ion source allows high ion beam current densities.
All ion gun parameters including accelerating voltage and cathode current are controlled automatically by a digital feedback loop, but they can always be changed manually during the sample preparation procedure. The initial values of the ion source parameters are set either automatically or manually and are continuously displayed on the computer screen.
 

The ion mills operating in the 150-2000 eV energy range are suitable for thinning of dimpled or mechanically polished thin (≤25µm) planar samples at ion energies ranging from 1000 to 2000eV.
 
Gentle Mill™3
The Gentle Mill™3 represents the third generation of Technoorg’s dedicated low-energy ion beam workstations. With its automated ion source setup, computer-aided gas flow control, easy to use graphical user interface and library of pre-programmed milling recipes. the GM3 offers a truly user-independent, fully automated thinning procedure for high-quality TEM sample preparation.
The Gentle Mill™3 has a Color CCD camera for full visual control and milling supervision with manual-zoom video lens of 50-400x magnification range. It has an auto-termination, either by detecting the perforation or monitoring the evolution of surface topography.
 

 model

Gentle Mill™ (IV5)

Gentle Mill™3 (IV8)

settings

manual

automated (or manual)

gas flow
control

via a needle valve enables manual optimization of the ion source performance

motorized needle valve control for automatic, user-independent ion source setup

milling
parameters

manual setting such as angle of beam incidence, speed and the oscillation angle of in-plane sample motion

Pre-programmed milling recipes for automatic setting of mechanical milling parameters
(manual adjustment also possible)

imaging
system

CCD camera with fixed magnification

high-resolution color CCD camera with manual zoom video lens of
50-400x magnification range

milling
process
termination

built-in timer function for termination of the milling procedure

 optical termination supported
by an image analysis module
(perforation or surface topography)

special
sample
holders

not available

 sample holders for
 • ion beam slope cutting
 • final polishing (EBSD samples)

Gentle Mill™3
Special Sample Holders for
Final Polishing (EBSD, OIM etc.) and Ion Beam Slope Cutting

Slope CuttingFinal Polishing

 specifications

Gentle Mill™ (IV5) and Gentle Mill™3 (IV8)

ion gun

patented "Hot-Cathode Low-Energy Ion Gun"

beam energy

150 eV - 2000 eV

beam diameter

750 - 1200 µm (FWHM)

 beam current

7 - 90 µA

milling angle

0° - 45° in 0.1° increments

sample mounting

Technoorg-designed titanium holder accepting TEM samples of thickness ranging from 40 to 200 µm

sample handling

load-lock system for fast specimen exchange

rotation

variable speed from 1 to 6 rpm

vacuum system

oil-free diaphragm and turbomolecular pumps with combined (Pirani/Penning) vacuum gauge

cooling system

closed-circuit cooling system and intelligent heat management concept, 1.5 liters of ion-exchanged or distilled water for the closed-circuit cooling system

gas supply system

Argon 5.0 (99.999%) or other noble gases of 1.4 - 1.7 bar absolute pressure